Investigation into machining performance of microstructurally engineered in-situ particle reinforced magnesium matrix composite S.K. Sahoo, B.N. Sahoo, S.K. Panigrahi Journal of Magnesium and Alloys, 2023 Magnesium and magnesium in-situ composites have significant potential in the application of design and manufacturing for automotive and aerospace industries because of their high specific strength and reduced fuel consumption. But there are many challenges for machining of Mg based alloys and composites because of the high tendency of fire and oxidation. These challenges can be minimized through microstructural engineering. In this present study, the machining performances of AZ91 Mg alloy and in-situ hybrid TiC+TiB2 reinforced AZ91 metal matrix composite was investigated. The effect β-Mg17Al12 phases and grain refinement with and without in-situ particles on machinability were studied through microstructural engineering via aging and friction stir processing. The end milling operation was carried out at different cutting speeds ranging from 25 mm/min to 90 mm/min under dry environment by using an AlTiN-coated tungsten carbide tool. The optimum cutting speed for machining was found to be 75 mm/min based on the surface roughness values of all conditioned materials. The base material with dendritic microstructure was found to have poor machinability in terms of inadequate surface finish and edge-burrs formation. The combined effect of in-situ TiC+TiB2 particles addition and grain refinement enhanced the machining performance of the material with superior surface finish, negligible edge-burr formation and better tool wear resistance. The influence of in-situ TiC+TiB2 particles, β-Mg17Al12 phases and grain refinement on machining characteristics are explained based on the tool wear mechanisms, chip behavior and machining induced affected zone.
Comparative study on high temperature deformation behavior and processing maps of Mg-4Zn-1RE-0.5Zr alloy with and without in-situ sub-micron sized TiB2 reinforcement S.K. Sahoo, S.K. Panigrahi Journal of Magnesium and Alloys, 2022 Mg-4Zn-1RE-0.5Zr (ZE41) Mg alloy is extensively used in the aerospace and automobile industries. In order to improve the applicability and performance, this alloy was engineered with in-situ TiB2 reinforcement to form TiB2/ZE41 composite. The high temperature deformation behavior and manufacturability of the newly developed TiB2/ZE41 composite and the parent ZE41 Mg alloy were studied via establishing constitutive modeling of flow stress, deformation activation energy and processing map over a temperature range of 250 °C - 450 °C and strain rate range of 0.001 s−1 - 10 s−1. The predicted flow stress behavior of both materials were found to be well consistent with the experimental values. A significant improvement in activation energy was found in TiB2/ZE41 composite (171.54 kJ/mol) as compared to the ZE41 alloy (148.15 kJ/mol) due to the dispersed strengthening of in-situ TiB2 particles. The processing maps were developed via dynamic material modeling. A wider workability domain and higher peak efficiency (45%) were observed in TiB2/ZE41 composite as compared to ZE41 alloy (41%). The Dynamic recrystallization is found to be the dominating deformation mechanism for both materials; however, particle stimulated nucleation was found to be an additional mode of deformation in TiB2/ZE41 composite. The twinning and stress induced cracks were observed in both the materials at low temperature and high strain rate. A narrow range of instability zone is found in the present TiB2/ZE41 composite among the existing published literature on Mg based composites. The detailed microstructural characterization was carried out in both workability and instability domains to establish the governing deformation mechanisms.